Sintesis surfaktan asid amino terasil-N daripada L-prolina Dan palmitoil klorida

Translated title of the contribution: Synthesis of n-acylated amino acid surfactant from l-proline and palmitoyl chloride

Meutia Fadhilah Hasibuan, Mohd Wahid Samsudin, Muhammad Rahimi Usop, Suria Ramli

Research output: Contribution to journalArticle

Abstract

A biodegradable, less toxic and environmentally friendly N-acylated amino acid surfactant was prepared from the amino acid L-proline and palmitoyl chloride through acylation reaction using the Schotten-Baumann reaction condition. The reaction result was a white flake form and the percentage of the crude yield was 72% with melting point in range of 52°C-58°C. Functional group of amide which was detected using Fourier Transform Infrared method showed the presence of N-palmitoyl proline. The purity analysis using High Performance Liquid Chromatography and Thin Layer Chromatography showed the result was a mixture compound.

Original languageUndefined/Unknown
Pages (from-to)230-235
Number of pages6
JournalMalaysian Journal of Analytical Sciences
Volume19
Issue number1
Publication statusPublished - 2015

Fingerprint

Proline
Surface-Active Agents
Amino Acids
Thin layer chromatography
Acylation
Poisons
High performance liquid chromatography
Amides
Functional groups
Melting point
Fourier transforms
Infrared radiation
palmitoyl chloride

Keywords

  • Amidation reaction
  • Biodegradable surfactant
  • N-acylated amino acids
  • Schotten-Baumann

ASJC Scopus subject areas

  • Analytical Chemistry

Cite this

Sintesis surfaktan asid amino terasil-N daripada L-prolina Dan palmitoil klorida. / Hasibuan, Meutia Fadhilah; Wahid Samsudin, Mohd; Usop, Muhammad Rahimi; Ramli, Suria.

In: Malaysian Journal of Analytical Sciences, Vol. 19, No. 1, 2015, p. 230-235.

Research output: Contribution to journalArticle

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