Synthesis and X-ray structure study of cis-trans 3-(3-biphenyl carbonylthioureido)propanoic acid(I) and N-(4-biphenyl carbonyl)-N -(3-hydroxyphenyl)thiourea(II)

Hamza M. Abosadiya, Salem El Ashoor, Bohari Mohd. Yamin

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

Benzoylthiourea derivatives can be synthesized from the reaction between benzoyl- isothiocyanate and amine compounds. Consequently, with a biphenyl carbonoyl derivative can be obtained. Both compounds I and II have been characterized by microelemental analysis, IR and X-ray diffraction. Single crystal X-ray investigation showed that the compounds crystallized in monocleinic system with space group of P21/c and the unit cell dimension for the compounds I and II are a = 21.819(5) Å, b = 4.8005(12) Å c = 15.539(4) Å, β =96.163(4) and a = 14.117(3) Å, b =7.0048(14) Å, c = 17.690(3) Å, β =107.960(3)°, respectively.

Original languageEnglish
Pages (from-to)572-576
Number of pages5
JournalRasayan Journal of Chemistry
Volume2
Issue number3
Publication statusPublished - Jul 2009

Fingerprint

Thiourea
Thioureas
X-Ray Diffraction
Amines
X-Rays
Derivatives
X rays
Acids
Single crystals
X ray diffraction
propionic acid
diphenyl
isothiocyanic acid

Keywords

  • Benzoyl-isothiocyanate
  • Benzoylthiourea
  • Microelemental analysis

ASJC Scopus subject areas

  • Chemistry(all)
  • Biochemistry
  • Chemical Engineering(all)
  • Pharmacology, Toxicology and Pharmaceutics(all)
  • Energy(all)

Cite this

Synthesis and X-ray structure study of cis-trans 3-(3-biphenyl carbonylthioureido)propanoic acid(I) and N-(4-biphenyl carbonyl)-N -(3-hydroxyphenyl)thiourea(II). / Abosadiya, Hamza M.; Ashoor, Salem El; Mohd. Yamin, Bohari.

In: Rasayan Journal of Chemistry, Vol. 2, No. 3, 07.2009, p. 572-576.

Research output: Contribution to journalArticle

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AB - Benzoylthiourea derivatives can be synthesized from the reaction between benzoyl- isothiocyanate and amine compounds. Consequently, with a biphenyl carbonoyl derivative can be obtained. Both compounds I and II have been characterized by microelemental analysis, IR and X-ray diffraction. Single crystal X-ray investigation showed that the compounds crystallized in monocleinic system with space group of P21/c and the unit cell dimension for the compounds I and II are a = 21.819(5) Å, b = 4.8005(12) Å c = 15.539(4) Å, β =96.163(4) and a = 14.117(3) Å, b =7.0048(14) Å, c = 17.690(3) Å, β =107.960(3)°, respectively.

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