Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

1,1'-Bis(2-bromobenzoylthioureido)ethane was synthesized from the reaction of 2-bromobenzoylisothiocyanate and ethylenediamine in acetonitrile. The compound was characterized by FT-IR, 1H, and 13C NMR spectroscopy techniques. Furthermor compound was found to crystallized in monoclinic system with space group of P2(1)/c. In each thiourea moiety the thiono group is trans to the benzoyl across their C-N bonds. The crystal structures are stabilized by N-H···S intermolecular hydrogen bonds to form infinite two dimensional network.

Original languageEnglish
Title of host publication2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium
PublisherAmerican Institute of Physics Inc.
Volume1784
ISBN (Electronic)9780735414464
DOIs
Publication statusPublished - 17 Nov 2016
Event2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016 - Selangor, Malaysia
Duration: 13 Apr 201614 Apr 2016

Other

Other2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016
CountryMalaysia
CitySelangor
Period13/4/1614/4/16

Fingerprint

ethane
crystal structure
thioureas
ethylenediamine
synthesis
acetonitrile
hydrogen bonds
nuclear magnetic resonance
spectroscopy

Keywords

  • Thiourea
  • X-ray crystallography

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Abosaadiya, S. M., Mohd. Yamin, B., & Hasbullah, S. A. (2016). Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium (Vol. 1784). [030009] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966747

Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane. / Abosaadiya, Salima M.; Mohd. Yamin, Bohari; Hasbullah, Siti Aishah.

2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016. 030009.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abosaadiya, SM, Mohd. Yamin, B & Hasbullah, SA 2016, Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane. in 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. vol. 1784, 030009, American Institute of Physics Inc., 2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016, Selangor, Malaysia, 13/4/16. https://doi.org/10.1063/1.4966747
Abosaadiya SM, Mohd. Yamin B, Hasbullah SA. Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784. American Institute of Physics Inc. 2016. 030009 https://doi.org/10.1063/1.4966747
Abosaadiya, Salima M. ; Mohd. Yamin, Bohari ; Hasbullah, Siti Aishah. / Synthesis and crystal structure of 1,1'-Bis(2-bromobenzoyl thioureido)ethane. 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016.
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