Abstract
Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.
| Original language | English |
|---|---|
| Title of host publication | 2018 UKM FST Postgraduate Colloquium |
| Subtitle of host publication | Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium |
| Editors | Noor Hayati Ahmad Rasol, Kamarulzaman Ibrahim, Siti Aishah Hasbullah, Mohammad Hafizuddin Hj. Jumali, Nazlina Ibrahim, Marlia Mohd Hanafiah, Mohd Talib Latif |
| Publisher | American Institute of Physics Inc. |
| ISBN (Electronic) | 9780735418431 |
| DOIs | |
| Publication status | Published - 27 Jun 2019 |
| Event | 2018 UKM FST Postgraduate Colloquium - Selangor, Malaysia Duration: 4 Apr 2018 → 6 Apr 2018 |
Publication series
| Name | AIP Conference Proceedings |
|---|---|
| Volume | 2111 |
| ISSN (Print) | 0094-243X |
| ISSN (Electronic) | 1551-7616 |
Conference
| Conference | 2018 UKM FST Postgraduate Colloquium |
|---|---|
| Country | Malaysia |
| City | Selangor |
| Period | 4/4/18 → 6/4/18 |
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ASJC Scopus subject areas
- Ecology, Evolution, Behavior and Systematics
- Ecology
- Plant Science
- Physics and Astronomy(all)
- Nature and Landscape Conservation
Cite this
Synthesis and characterization of nickel and cobalt species within SBA-15. / Kamaruzaman, Muhammad Fadhli; Hin, Taufiq Yap Yun; Derawi, Darfizzi.
2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium. ed. / Noor Hayati Ahmad Rasol; Kamarulzaman Ibrahim; Siti Aishah Hasbullah; Mohammad Hafizuddin Hj. Jumali; Nazlina Ibrahim; Marlia Mohd Hanafiah; Mohd Talib Latif. American Institute of Physics Inc., 2019. 050007 (AIP Conference Proceedings; Vol. 2111).Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - Synthesis and characterization of nickel and cobalt species within SBA-15
AU - Kamaruzaman, Muhammad Fadhli
AU - Hin, Taufiq Yap Yun
AU - Derawi, Darfizzi
PY - 2019/6/27
Y1 - 2019/6/27
N2 - Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.
AB - Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.
UR - http://www.scopus.com/inward/record.url?scp=85068453705&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85068453705&partnerID=8YFLogxK
U2 - 10.1063/1.5111255
DO - 10.1063/1.5111255
M3 - Conference contribution
T3 - AIP Conference Proceedings
BT - 2018 UKM FST Postgraduate Colloquium
A2 - Rasol, Noor Hayati Ahmad
A2 - Ibrahim, Kamarulzaman
A2 - Hasbullah, Siti Aishah
A2 - Jumali, Mohammad Hafizuddin Hj.
A2 - Ibrahim, Nazlina
A2 - Hanafiah, Marlia Mohd
A2 - Latif, Mohd Talib
PB - American Institute of Physics Inc.
ER -