Synthesis and characterization of nickel and cobalt species within SBA-15

Muhammad Fadhli Kamaruzaman, Taufiq Yap Yun Hin, Darfizzi Derawi

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.

Original languageEnglish
Title of host publication2018 UKM FST Postgraduate Colloquium
Subtitle of host publicationProceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium
EditorsNoor Hayati Ahmad Rasol, Kamarulzaman Ibrahim, Siti Aishah Hasbullah, Mohammad Hafizuddin Hj. Jumali, Nazlina Ibrahim, Marlia Mohd Hanafiah, Mohd Talib Latif
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735418431
DOIs
Publication statusPublished - 27 Jun 2019
Event2018 UKM FST Postgraduate Colloquium - Selangor, Malaysia
Duration: 4 Apr 20186 Apr 2018

Publication series

NameAIP Conference Proceedings
Volume2111
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference2018 UKM FST Postgraduate Colloquium
CountryMalaysia
CitySelangor
Period4/4/186/4/18

Fingerprint

cobalt
nickel
catalysts
catalyst
synthesis
isotherm
isotherms
metals
desorption
silica
roasting
moisture content
oxides
metal oxides
transmission electron microscopy
adsorption
X-ray diffraction
silicon dioxide
metal
cells

ASJC Scopus subject areas

  • Ecology, Evolution, Behavior and Systematics
  • Ecology
  • Plant Science
  • Physics and Astronomy(all)
  • Nature and Landscape Conservation

Cite this

Kamaruzaman, M. F., Hin, T. Y. Y., & Derawi, D. (2019). Synthesis and characterization of nickel and cobalt species within SBA-15. In N. H. A. Rasol, K. Ibrahim, S. A. Hasbullah, M. H. H. Jumali, N. Ibrahim, M. M. Hanafiah, & M. T. Latif (Eds.), 2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium [050007] (AIP Conference Proceedings; Vol. 2111). American Institute of Physics Inc.. https://doi.org/10.1063/1.5111255

Synthesis and characterization of nickel and cobalt species within SBA-15. / Kamaruzaman, Muhammad Fadhli; Hin, Taufiq Yap Yun; Derawi, Darfizzi.

2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium. ed. / Noor Hayati Ahmad Rasol; Kamarulzaman Ibrahim; Siti Aishah Hasbullah; Mohammad Hafizuddin Hj. Jumali; Nazlina Ibrahim; Marlia Mohd Hanafiah; Mohd Talib Latif. American Institute of Physics Inc., 2019. 050007 (AIP Conference Proceedings; Vol. 2111).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Kamaruzaman, MF, Hin, TYY & Derawi, D 2019, Synthesis and characterization of nickel and cobalt species within SBA-15. in NHA Rasol, K Ibrahim, SA Hasbullah, MHH Jumali, N Ibrahim, MM Hanafiah & MT Latif (eds), 2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium., 050007, AIP Conference Proceedings, vol. 2111, American Institute of Physics Inc., 2018 UKM FST Postgraduate Colloquium, Selangor, Malaysia, 4/4/18. https://doi.org/10.1063/1.5111255
Kamaruzaman MF, Hin TYY, Derawi D. Synthesis and characterization of nickel and cobalt species within SBA-15. In Rasol NHA, Ibrahim K, Hasbullah SA, Jumali MHH, Ibrahim N, Hanafiah MM, Latif MT, editors, 2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium. American Institute of Physics Inc. 2019. 050007. (AIP Conference Proceedings). https://doi.org/10.1063/1.5111255
Kamaruzaman, Muhammad Fadhli ; Hin, Taufiq Yap Yun ; Derawi, Darfizzi. / Synthesis and characterization of nickel and cobalt species within SBA-15. 2018 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2018 Postgraduate Colloquium. editor / Noor Hayati Ahmad Rasol ; Kamarulzaman Ibrahim ; Siti Aishah Hasbullah ; Mohammad Hafizuddin Hj. Jumali ; Nazlina Ibrahim ; Marlia Mohd Hanafiah ; Mohd Talib Latif. American Institute of Physics Inc., 2019. (AIP Conference Proceedings).
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N2 - Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.

AB - Mesoporous silica SBA-15 was synthesized according to Zhao method. A mono and bimetallic of nickel/cobalt metal was successfully loaded into mesoporous SBA-15 to form 5% Co/SBA-15, 5% Ni/SBA-15 and 2.5%-2.5% Ni-Co/SBA-15. All the impregnated SBA-15 were synthesized via wetness impregnation method. After calcination, both nickel and cobalt present in the form of metal oxide of NiO and Co3O4. The low angle XRD analysis showed that all the synthesized catalyst possessed a hexagonal unit cell reflection of short channeled SBA-15. The mesoporous structure also was well preserved even after Ni and Co loading. This result was agreed with the N2 adsorption-desorption isotherm analysis which indicated all catalysts have type IV isotherm. In addition, the TEM analysis also proved the presence of hexagonal channels in all synthesized catalysts.

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