Synthesis and characterization of MN2+ doped ZnS using reverse miceller method

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

In this work we synthesized the monodisperse of Zn1-xMnxS with x =0.00,0.02,0.04,0.06,0.08 and 0.10 nanoparticles by reverse micelle method using sodium bis(2- ethylhexyl) sulfosuccinate (AOT) as surfactant. The prepared particles were characterized using UV-Visible Spectroscopy, X-ray diffraction (XRD), Transmission Electron Microscopy (TEM) and Photoluminescence (PL) for size, morphology and optical of the samples. UV-vis absorbance spectra for all of the synthesized nanoparticles show the maximum absorption for all samples is observed at range 210 - 300 nm. The absorption edge shifted to lower wavelengths when doping with ion Mn as per UV-Vis spectroscopy. The band gap energy values were increase from 4.50eV to 4.90 eV. This blue shift is attributed to the quantum confinement effect. The size of particles is found to be 3-5nm range. The Mn2+ doped ZnS nanoparticles using reverse micelles method shows the enhance of PL intensity results in monodisperse nanoparticles.

Original languageEnglish
Title of host publicationAdvanced Materials Research
PublisherTrans Tech Publications Ltd
Pages283-287
Number of pages5
Volume970
ISBN (Print)9783038350927
DOIs
Publication statusPublished - 2014
Event1st International Conference on Science and Engineering of Materials, ICoSEM 2013 - Kuala Lumpur
Duration: 13 Nov 201314 Nov 2013

Publication series

NameAdvanced Materials Research
Volume970
ISSN (Print)10226680
ISSN (Electronic)16628985

Other

Other1st International Conference on Science and Engineering of Materials, ICoSEM 2013
CityKuala Lumpur
Period13/11/1314/11/13

Fingerprint

Micelles
Nanoparticles
Photoluminescence
Quantum confinement
Ultraviolet spectroscopy
Energy gap
Surface active agents
Sodium
Doping (additives)
Spectroscopy
Transmission electron microscopy
X ray diffraction
Wavelength
Ions

Keywords

  • Nanoparticles
  • Photoluminescence
  • Quantum confinement effect
  • UV-vis absorbance spectra

ASJC Scopus subject areas

  • Engineering(all)

Cite this

Ibrahim, R. M., Markom, M., & Abdullah, H. (2014). Synthesis and characterization of MN2+ doped ZnS using reverse miceller method. In Advanced Materials Research (Vol. 970, pp. 283-287). (Advanced Materials Research; Vol. 970). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/AMR.970.283

Synthesis and characterization of MN2+ doped ZnS using reverse miceller method. / Ibrahim, R. M.; Markom, Masturah; Abdullah, Huda.

Advanced Materials Research. Vol. 970 Trans Tech Publications Ltd, 2014. p. 283-287 (Advanced Materials Research; Vol. 970).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Ibrahim, RM, Markom, M & Abdullah, H 2014, Synthesis and characterization of MN2+ doped ZnS using reverse miceller method. in Advanced Materials Research. vol. 970, Advanced Materials Research, vol. 970, Trans Tech Publications Ltd, pp. 283-287, 1st International Conference on Science and Engineering of Materials, ICoSEM 2013, Kuala Lumpur, 13/11/13. https://doi.org/10.4028/www.scientific.net/AMR.970.283
Ibrahim RM, Markom M, Abdullah H. Synthesis and characterization of MN2+ doped ZnS using reverse miceller method. In Advanced Materials Research. Vol. 970. Trans Tech Publications Ltd. 2014. p. 283-287. (Advanced Materials Research). https://doi.org/10.4028/www.scientific.net/AMR.970.283
Ibrahim, R. M. ; Markom, Masturah ; Abdullah, Huda. / Synthesis and characterization of MN2+ doped ZnS using reverse miceller method. Advanced Materials Research. Vol. 970 Trans Tech Publications Ltd, 2014. pp. 283-287 (Advanced Materials Research).
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