Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

A new route to the synthesis of maleimide is described. 2-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)acetic acid maleimide (1) and 2-(4-(2,5-Dioxo-2,5-dihydro- 1H-pyrrol-1-yl)phenyl)ethanoic acid maleimide (2) have been synthesized by the reaction of maleic anhydride with glycine and 4-aminophenyl acetic aicd. Maleimide (1) was synthesized by conventional technique while maleimide (2) was synthesized by microwave method. The compounds were characterized using FT-Infrared (FT-IR), 1H and 13C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry.

Original languageEnglish
Title of host publication2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium
PublisherAmerican Institute of Physics Inc.
Volume1784
ISBN (Electronic)9780735414464
DOIs
Publication statusPublished - 17 Nov 2016
Event2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016 - Selangor, Malaysia
Duration: 13 Apr 201614 Apr 2016

Other

Other2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016
CountryMalaysia
CitySelangor
Period13/4/1614/4/16

Fingerprint

magnetic resonance spectroscopy
anhydrides
glycine
acetic acid
mass spectroscopy
routes
microwaves
nuclear magnetic resonance
acids
synthesis
spectroscopy

Keywords

  • maleimide derivative
  • microwave reaction

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Poad, S. N. M., Hassan, N. I., & Hassan, N. H. (2016). Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium (Vol. 1784). [030016] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966754

Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide. / Poad, Siti Nashwa Mohd; Hassan, Nurul Izzaty; Hassan, Nur Hasyareeda.

2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016. 030016.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Poad, SNM, Hassan, NI & Hassan, NH 2016, Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide. in 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. vol. 1784, 030016, American Institute of Physics Inc., 2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016, Selangor, Malaysia, 13/4/16. https://doi.org/10.1063/1.4966754
Poad SNM, Hassan NI, Hassan NH. Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784. American Institute of Physics Inc. 2016. 030016 https://doi.org/10.1063/1.4966754
Poad, Siti Nashwa Mohd ; Hassan, Nurul Izzaty ; Hassan, Nur Hasyareeda. / Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide. 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016.
@inproceedings{f0c7583762224721a221d6693f3e7c90,
title = "Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide",
abstract = "A new route to the synthesis of maleimide is described. 2-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)acetic acid maleimide (1) and 2-(4-(2,5-Dioxo-2,5-dihydro- 1H-pyrrol-1-yl)phenyl)ethanoic acid maleimide (2) have been synthesized by the reaction of maleic anhydride with glycine and 4-aminophenyl acetic aicd. Maleimide (1) was synthesized by conventional technique while maleimide (2) was synthesized by microwave method. The compounds were characterized using FT-Infrared (FT-IR), 1H and 13C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry.",
keywords = "maleimide derivative, microwave reaction",
author = "Poad, {Siti Nashwa Mohd} and Hassan, {Nurul Izzaty} and Hassan, {Nur Hasyareeda}",
year = "2016",
month = "11",
day = "17",
doi = "10.1063/1.4966754",
language = "English",
volume = "1784",
booktitle = "2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium",
publisher = "American Institute of Physics Inc.",

}

TY - GEN

T1 - Synthesis and characterization of acetic acid and ethanoic acid (based)-maleimide

AU - Poad, Siti Nashwa Mohd

AU - Hassan, Nurul Izzaty

AU - Hassan, Nur Hasyareeda

PY - 2016/11/17

Y1 - 2016/11/17

N2 - A new route to the synthesis of maleimide is described. 2-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)acetic acid maleimide (1) and 2-(4-(2,5-Dioxo-2,5-dihydro- 1H-pyrrol-1-yl)phenyl)ethanoic acid maleimide (2) have been synthesized by the reaction of maleic anhydride with glycine and 4-aminophenyl acetic aicd. Maleimide (1) was synthesized by conventional technique while maleimide (2) was synthesized by microwave method. The compounds were characterized using FT-Infrared (FT-IR), 1H and 13C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry.

AB - A new route to the synthesis of maleimide is described. 2-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)acetic acid maleimide (1) and 2-(4-(2,5-Dioxo-2,5-dihydro- 1H-pyrrol-1-yl)phenyl)ethanoic acid maleimide (2) have been synthesized by the reaction of maleic anhydride with glycine and 4-aminophenyl acetic aicd. Maleimide (1) was synthesized by conventional technique while maleimide (2) was synthesized by microwave method. The compounds were characterized using FT-Infrared (FT-IR), 1H and 13C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry.

KW - maleimide derivative

KW - microwave reaction

UR - http://www.scopus.com/inward/record.url?scp=85014709701&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=85014709701&partnerID=8YFLogxK

U2 - 10.1063/1.4966754

DO - 10.1063/1.4966754

M3 - Conference contribution

AN - SCOPUS:85014709701

VL - 1784

BT - 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium

PB - American Institute of Physics Inc.

ER -