Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

New mono-thiourea derivative, 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea (3) has been synthesized from the reaction of 1-naphthyl isothiocyanate (1) and 1,3-phenylenediamine (2) using conventional method. The percentage yield of compound 3 was 82%. The compound 3 was characterized using FT-Infrared (FT-IR), 1H and 1C Nuclear Magnetic Resonance (NMR) spectroscopies and Mass Spectrometry. An application of chemical sensor on this compound was prepared and examined by UV-vis spectrometer to study the binding interaction between metal ions and compound 3.

Original languageEnglish
Title of host publication2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium
PublisherAmerican Institute of Physics Inc.
Volume1784
ISBN (Electronic)9780735414464
DOIs
Publication statusPublished - 17 Nov 2016
Event2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016 - Selangor, Malaysia
Duration: 13 Apr 201614 Apr 2016

Other

Other2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016
CountryMalaysia
CitySelangor
Period13/4/1614/4/16

Fingerprint

thioureas
metal ions
metal compounds
magnetic resonance spectroscopy
synthesis
mass spectroscopy
spectrometers
nuclear magnetic resonance
sensors
spectroscopy
interactions

Keywords

  • Binding study
  • Metal ions
  • Mono-thiourea

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Ngah, F. A. A., Lee, Y. H., Hassan, N. I., & Hasbullah, S. A. (2016). Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium (Vol. 1784). [030014] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966752

Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions. / Ngah, Fatimatul Akma Awang; Lee, Yook Heng; Hassan, Nurul Izzaty; Hasbullah, Siti Aishah.

2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016. 030014.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Ngah, FAA, Lee, YH, Hassan, NI & Hasbullah, SA 2016, Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions. in 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. vol. 1784, 030014, American Institute of Physics Inc., 2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016, Selangor, Malaysia, 13/4/16. https://doi.org/10.1063/1.4966752
Ngah FAA, Lee YH, Hassan NI, Hasbullah SA. Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784. American Institute of Physics Inc. 2016. 030014 https://doi.org/10.1063/1.4966752
Ngah, Fatimatul Akma Awang ; Lee, Yook Heng ; Hassan, Nurul Izzaty ; Hasbullah, Siti Aishah. / Synthesis and characterization of 1-(3-aminophenyl)-3-(naphthalen-1-yl)thiourea and preliminary study towards binding with metal ions. 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016.
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