Abstract
β-ketoamine ligands are important members of heterodonor ligand because of their ease of preparation and modification of both steric and/or electronic effects. Complexes with β-ketoamine has received much less attention and there has been no study about this complex with β-ketoamine in ionic liquid reported. Two type of β-ketoamine ligands which are 4-Amino-3-pentene-2-onato (A) and 3-Amino-2-butenoic acid methyl ester (B) have been synthesized in this work. The resulting compound formed was characterized using standard spectroscopic and structural techniques which includes 1H and 13C, NMR spectroscopy and FTIR spectroscopy. The 1H and 13C NMR spectrum displayed all the expected signals with correct integration and multiplicity. And it is proved that there are some differences between two ligands as observed in NMR and FTIR spectrum.
| Original language | English |
|---|---|
| Title of host publication | 2017 UKM FST Postgraduate Colloquium |
| Subtitle of host publication | Proceedings of the University Kebangsaan Malaysia, Faculty of Science and Technology 2017 Postgraduate Colloquium |
| Publisher | American Institute of Physics Inc. |
| Volume | 1940 |
| ISBN (Electronic) | 9780735416321 |
| DOIs | |
| Publication status | Published - 4 Apr 2018 |
| Event | 2017 UKM FST Postgraduate Colloquium - Selangor, Malaysia Duration: 12 Jul 2017 → 13 Jul 2017 |
Other
| Other | 2017 UKM FST Postgraduate Colloquium |
|---|---|
| Country | Malaysia |
| City | Selangor |
| Period | 12/7/17 → 13/7/17 |
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ASJC Scopus subject areas
- Physics and Astronomy(all)
Cite this
Synthesis and characterization β-ketoamine ligands. / Zaid, Nurzati Amani Mohamed; Hassan, Nur Hasyareeda; Abd Karim, Nurul Huda.
2017 UKM FST Postgraduate Colloquium: Proceedings of the University Kebangsaan Malaysia, Faculty of Science and Technology 2017 Postgraduate Colloquium. Vol. 1940 American Institute of Physics Inc., 2018. 020097.Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - Synthesis and characterization β-ketoamine ligands
AU - Zaid, Nurzati Amani Mohamed
AU - Hassan, Nur Hasyareeda
AU - Abd Karim, Nurul Huda
PY - 2018/4/4
Y1 - 2018/4/4
N2 - β-ketoamine ligands are important members of heterodonor ligand because of their ease of preparation and modification of both steric and/or electronic effects. Complexes with β-ketoamine has received much less attention and there has been no study about this complex with β-ketoamine in ionic liquid reported. Two type of β-ketoamine ligands which are 4-Amino-3-pentene-2-onato (A) and 3-Amino-2-butenoic acid methyl ester (B) have been synthesized in this work. The resulting compound formed was characterized using standard spectroscopic and structural techniques which includes 1H and 13C, NMR spectroscopy and FTIR spectroscopy. The 1H and 13C NMR spectrum displayed all the expected signals with correct integration and multiplicity. And it is proved that there are some differences between two ligands as observed in NMR and FTIR spectrum.
AB - β-ketoamine ligands are important members of heterodonor ligand because of their ease of preparation and modification of both steric and/or electronic effects. Complexes with β-ketoamine has received much less attention and there has been no study about this complex with β-ketoamine in ionic liquid reported. Two type of β-ketoamine ligands which are 4-Amino-3-pentene-2-onato (A) and 3-Amino-2-butenoic acid methyl ester (B) have been synthesized in this work. The resulting compound formed was characterized using standard spectroscopic and structural techniques which includes 1H and 13C, NMR spectroscopy and FTIR spectroscopy. The 1H and 13C NMR spectrum displayed all the expected signals with correct integration and multiplicity. And it is proved that there are some differences between two ligands as observed in NMR and FTIR spectrum.
UR - http://www.scopus.com/inward/record.url?scp=85045657195&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85045657195&partnerID=8YFLogxK
U2 - 10.1063/1.5028012
DO - 10.1063/1.5028012
M3 - Conference contribution
AN - SCOPUS:85045657195
VL - 1940
BT - 2017 UKM FST Postgraduate Colloquium
PB - American Institute of Physics Inc.
ER -