Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film

N. E S Sazali, Mohamad Deraman, Ramli Omar, Mohd. Amir Radhi Othman, M. Suleman, Siti Aisyah Shamsudin, N. S M Tajuddin, M. F Y M Hanappi, E. Hamdan, N. S M Nor, N. H. Basri

Research output: Chapter in Book/Report/Conference proceedingConference contribution

2 Citations (Scopus)

Abstract

In this study, we report the preparation of turbostratic-carbon/graphene from biomass amylose film by carbonization (N2 gas) and activation (CO2 gas) over different temperatures 600, 700, 800, 900, and 1000°C, respectively. The Raman spectroscopy results of the produced samples show that the values of the ID/IG ratio ranging from 0.75 to 0.99 are comparable to that of the commercial multilayer graphene and KOH treated multilayer graphene. The X-ray diffraction results of the produced samples show that a small decrease in the d002 (∼0.62 %) and d100 (∼0.57 %) values and a larger decrease in Lc (∼8.6 %) and La (∼27.2 %) values occurs as the carbonization and activation temperature increases, indicating that the increase in temperature has an effect on the growth of microcrystallites during carbonization and activation. This study demonstrates the potential of the amylose film to be used as a precursor for producing graphene flakes.

Original languageEnglish
Title of host publication2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium
PublisherAmerican Institute of Physics Inc.
Volume1784
ISBN (Electronic)9780735414464
DOIs
Publication statusPublished - 17 Nov 2016
Event2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016 - Selangor, Malaysia
Duration: 13 Apr 201614 Apr 2016

Other

Other2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016
CountryMalaysia
CitySelangor
Period13/4/1614/4/16

Fingerprint

carbonization
graphene
preparation
carbon
activation
flakes
biomass
gases
temperature
Raman spectroscopy
diffraction
x rays

Keywords

  • Amylose film
  • Graphene
  • Raman spectroscopy
  • Specific capacitance
  • Supercapacitor
  • Turbostratic carbon
  • X-ray diffraction

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Sazali, N. E. S., Deraman, M., Omar, R., Othman, M. A. R., Suleman, M., Shamsudin, S. A., ... Basri, N. H. (2016). Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium (Vol. 1784). [040009] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966795

Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film. / Sazali, N. E S; Deraman, Mohamad; Omar, Ramli; Othman, Mohd. Amir Radhi; Suleman, M.; Shamsudin, Siti Aisyah; Tajuddin, N. S M; Hanappi, M. F Y M; Hamdan, E.; Nor, N. S M; Basri, N. H.

2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016. 040009.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Sazali, NES, Deraman, M, Omar, R, Othman, MAR, Suleman, M, Shamsudin, SA, Tajuddin, NSM, Hanappi, MFYM, Hamdan, E, Nor, NSM & Basri, NH 2016, Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film. in 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. vol. 1784, 040009, American Institute of Physics Inc., 2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016, Selangor, Malaysia, 13/4/16. https://doi.org/10.1063/1.4966795
Sazali NES, Deraman M, Omar R, Othman MAR, Suleman M, Shamsudin SA et al. Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film. In 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784. American Institute of Physics Inc. 2016. 040009 https://doi.org/10.1063/1.4966795
Sazali, N. E S ; Deraman, Mohamad ; Omar, Ramli ; Othman, Mohd. Amir Radhi ; Suleman, M. ; Shamsudin, Siti Aisyah ; Tajuddin, N. S M ; Hanappi, M. F Y M ; Hamdan, E. ; Nor, N. S M ; Basri, N. H. / Preparation and structural characterization of turbostratic-carbon/graphene derived from amylose film. 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784 American Institute of Physics Inc., 2016.
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