N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine

Dhafer S. Zinad, Dunya L. Al-Duhaidahaw, Ahmed Al-Amiery, Abdul Amir H. Kadhum

Research output: Contribution to journalArticle

Abstract

N-[4-(1-Methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2 -chloro-4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) ( 1 H-NMR and 13 C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high-performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.

Original languageEnglish
Article numberM1030
JournalMolBank
Volume2018
Issue number4
DOIs
Publication statusPublished - 1 Dec 2018

Fingerprint

4-methylimidazole
Diamines
diamines
Benzene
imidazoles
Magnetic Resonance Spectroscopy
benzene
Nuclear magnetic resonance
nuclear magnetic resonance
Mass spectrometry
mass spectroscopy
thin layer chromatography
Thin layer chromatography
liquid chromatography
High performance liquid chromatography
gas chromatography
Thin Layer Chromatography
Chemical analysis
chemical analysis
Gas chromatography

Keywords

  • 4-phenylenediamine
  • Bipyridine
  • Butanol
  • Fluorescent
  • Imidazole

ASJC Scopus subject areas

  • Biochemistry
  • Physical and Theoretical Chemistry
  • Organic Chemistry

Cite this

Zinad, D. S., Al-Duhaidahaw, D. L., Al-Amiery, A., & Kadhum, A. A. H. (2018). N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine MolBank, 2018(4), [M1030]. https://doi.org/10.3390/M1030

N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine . / Zinad, Dhafer S.; Al-Duhaidahaw, Dunya L.; Al-Amiery, Ahmed; Kadhum, Abdul Amir H.

In: MolBank, Vol. 2018, No. 4, M1030, 01.12.2018.

Research output: Contribution to journalArticle

Zinad, DS, Al-Duhaidahaw, DL, Al-Amiery, A & Kadhum, AAH 2018, ' N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine ', MolBank, vol. 2018, no. 4, M1030. https://doi.org/10.3390/M1030
Zinad DS, Al-Duhaidahaw DL, Al-Amiery A, Kadhum AAH. N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine MolBank. 2018 Dec 1;2018(4). M1030. https://doi.org/10.3390/M1030
Zinad, Dhafer S. ; Al-Duhaidahaw, Dunya L. ; Al-Amiery, Ahmed ; Kadhum, Abdul Amir H. / N-[4-(1-methyl-1H-imidazol-2-yl)-2,4 -bipyridin-2 -yl]benzene-1,4-diamine In: MolBank. 2018 ; Vol. 2018, No. 4.
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AU - Al-Duhaidahaw, Dunya L.

AU - Al-Amiery, Ahmed

AU - Kadhum, Abdul Amir H.

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N2 - N-[4-(1-Methyl-1H-imidazol-2-yl)-2,4 ′ -bipyridin-2 ′ -yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2 ′ -chloro-4-(1-methyl-1H-imidazol-2-yl)-2,4 ′ -bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) ( 1 H-NMR and 13 C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high-performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.

AB - N-[4-(1-Methyl-1H-imidazol-2-yl)-2,4 ′ -bipyridin-2 ′ -yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2 ′ -chloro-4-(1-methyl-1H-imidazol-2-yl)-2,4 ′ -bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) ( 1 H-NMR and 13 C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high-performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.

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