Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis

R. Rafiee-Moghaddam, Jumat Salimon, Md Jelas Haron, H. Jahangirian

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio of 6/1 of methyl hydroxylamine/oil, temperature at 41°C, enzyme 30mg/mmol and 72 h of reaction time. At this optimal condition, the yield% of methyl fatty hydroxamic based on Jatropha Curcas seed oil was 93.92%. The product was characterized by Fourier transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (1H-NMR and 13C NMR) spectra.

Original languageEnglish
Pages (from-to)415-422
Number of pages8
JournalDigest Journal of Nanomaterials and Biostructures
Volume8
Publication statusPublished - 2013

Fingerprint

Jatropha
Oilseeds
seeds
Seeds
Oils
oils
Nuclear magnetic resonance
nuclear magnetic resonance
Substrates
Hydroxamic Acids
Hydroxylamine
Fourier Analysis
fatty acids
Fatty acids
reaction time
Protons
enzymes
Fourier transforms
Magnetic Resonance Spectroscopy
Fatty Acids

Keywords

  • Enzymatic reaction
  • Jatropha curcas seed oil
  • Lipase
  • Methyl fatty hydroxamic acid

ASJC Scopus subject areas

  • Materials Science(all)
  • Biomedical Engineering
  • Physical and Theoretical Chemistry
  • Condensed Matter Physics
  • Structural Biology
  • Atomic and Molecular Physics, and Optics

Cite this

Rafiee-Moghaddam, R., Salimon, J., Haron, M. J., & Jahangirian, H. (2013). Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis. Digest Journal of Nanomaterials and Biostructures, 8, 415-422.

Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis. / Rafiee-Moghaddam, R.; Salimon, Jumat; Haron, Md Jelas; Jahangirian, H.

In: Digest Journal of Nanomaterials and Biostructures, Vol. 8, 2013, p. 415-422.

Research output: Contribution to journalArticle

Rafiee-Moghaddam, R, Salimon, J, Haron, MJ & Jahangirian, H 2013, 'Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis', Digest Journal of Nanomaterials and Biostructures, vol. 8, pp. 415-422.
Rafiee-Moghaddam, R. ; Salimon, Jumat ; Haron, Md Jelas ; Jahangirian, H. / Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis. In: Digest Journal of Nanomaterials and Biostructures. 2013 ; Vol. 8. pp. 415-422.
@article{3580173f90ae4b6b8dfe863e00e829a3,
title = "Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis",
abstract = "Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio of 6/1 of methyl hydroxylamine/oil, temperature at 41°C, enzyme 30mg/mmol and 72 h of reaction time. At this optimal condition, the yield{\%} of methyl fatty hydroxamic based on Jatropha Curcas seed oil was 93.92{\%}. The product was characterized by Fourier transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (1H-NMR and 13C NMR) spectra.",
keywords = "Enzymatic reaction, Jatropha curcas seed oil, Lipase, Methyl fatty hydroxamic acid",
author = "R. Rafiee-Moghaddam and Jumat Salimon and Haron, {Md Jelas} and H. Jahangirian",
year = "2013",
language = "English",
volume = "8",
pages = "415--422",
journal = "Digest Journal of Nanomaterials and Biostructures",
issn = "1842-3582",
publisher = "National Institute R and D of Materials Physics",

}

TY - JOUR

T1 - Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis

AU - Rafiee-Moghaddam, R.

AU - Salimon, Jumat

AU - Haron, Md Jelas

AU - Jahangirian, H.

PY - 2013

Y1 - 2013

N2 - Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio of 6/1 of methyl hydroxylamine/oil, temperature at 41°C, enzyme 30mg/mmol and 72 h of reaction time. At this optimal condition, the yield% of methyl fatty hydroxamic based on Jatropha Curcas seed oil was 93.92%. The product was characterized by Fourier transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (1H-NMR and 13C NMR) spectra.

AB - Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio of 6/1 of methyl hydroxylamine/oil, temperature at 41°C, enzyme 30mg/mmol and 72 h of reaction time. At this optimal condition, the yield% of methyl fatty hydroxamic based on Jatropha Curcas seed oil was 93.92%. The product was characterized by Fourier transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (1H-NMR and 13C NMR) spectra.

KW - Enzymatic reaction

KW - Jatropha curcas seed oil

KW - Lipase

KW - Methyl fatty hydroxamic acid

UR - http://www.scopus.com/inward/record.url?scp=84874293957&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84874293957&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:84874293957

VL - 8

SP - 415

EP - 422

JO - Digest Journal of Nanomaterials and Biostructures

JF - Digest Journal of Nanomaterials and Biostructures

SN - 1842-3582

ER -