Influence of iron oxide nano particles on electrospun poly (vinylidene fluride)-based carbon nanofibers on hydrogen storage

Samaneh Shahgaldi, Zahira Yaakob, Norazrina Mat Jali, Dariush Jafar Khadem, Wan Ramli Wan Daud, Edy Herianto

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Citation (Scopus)

Abstract

Electrospun Poly (vinylidene fluoride) (PVdF) fine fiber of 100-300 nm in diameter in ribbon shape was synthesized through the electrospinning process via sol-gel. In order to synthesize infusible nanofibers all processing of dehydrofluorination and carbonization was investigated. Iron nanoparticles was doped with PVDF nanofibers in order to be effective in surface area, and porosity to increase the hydrogen storage. The composition, morphology, structure and surface area of PVDF/Iron Oxide nanofibers were investigated by thermo gravimetric analysis (TGA) to determinate the temperature of possible decomposition and crystallinity, scanning electron microscopy (SEM), transmission electron microscopy (TEM), Micromeritics (ASAP2020) used to study the textural properties of the sample, like surface area, total pore volume, and micro pore volume. The result shows that the PVDF without dehydrofluorination treatment for infusibility become melt at around 160 °C. By adding the iron oxide nanoparticles as a catalyst it can improve the characteristic of the carbon fiber for hydrogen storage. In best of our knowledge, PVDF doping with iron oxide investigated for first time.

Original languageEnglish
Title of host publicationKey Engineering Materials
Pages1184-1189
Number of pages6
Volume471-472
DOIs
Publication statusPublished - 2011
Event8th International Conference on Composite Science and Technology, ICCST8 - Kuala Lumpur
Duration: 22 Mar 201124 Mar 2011

Publication series

NameKey Engineering Materials
Volume471-472
ISSN (Print)10139826

Other

Other8th International Conference on Composite Science and Technology, ICCST8
CityKuala Lumpur
Period22/3/1124/3/11

Fingerprint

Carbon nanofibers
Hydrogen storage
Nanofibers
Iron oxides
Nanoparticles
Carbonization
Electrospinning
Carbon fibers
Sol-gels
Thermogravimetric analysis
Porosity
Doping (additives)
Iron
Transmission electron microscopy
Decomposition
Scanning electron microscopy
Catalysts
Fibers
Processing
Chemical analysis

Keywords

  • Carbon nanofibers
  • Dehydrofluorination
  • Iron oxide
  • PVDF

ASJC Scopus subject areas

  • Materials Science(all)
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Shahgaldi, S., Yaakob, Z., Jali, N. M., Khadem, D. J., Wan Daud, W. R., & Herianto, E. (2011). Influence of iron oxide nano particles on electrospun poly (vinylidene fluride)-based carbon nanofibers on hydrogen storage. In Key Engineering Materials (Vol. 471-472, pp. 1184-1189). (Key Engineering Materials; Vol. 471-472). https://doi.org/10.4028/www.scientific.net/KEM.471-472.1184

Influence of iron oxide nano particles on electrospun poly (vinylidene fluride)-based carbon nanofibers on hydrogen storage. / Shahgaldi, Samaneh; Yaakob, Zahira; Jali, Norazrina Mat; Khadem, Dariush Jafar; Wan Daud, Wan Ramli; Herianto, Edy.

Key Engineering Materials. Vol. 471-472 2011. p. 1184-1189 (Key Engineering Materials; Vol. 471-472).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Shahgaldi, S, Yaakob, Z, Jali, NM, Khadem, DJ, Wan Daud, WR & Herianto, E 2011, Influence of iron oxide nano particles on electrospun poly (vinylidene fluride)-based carbon nanofibers on hydrogen storage. in Key Engineering Materials. vol. 471-472, Key Engineering Materials, vol. 471-472, pp. 1184-1189, 8th International Conference on Composite Science and Technology, ICCST8, Kuala Lumpur, 22/3/11. https://doi.org/10.4028/www.scientific.net/KEM.471-472.1184
Shahgaldi, Samaneh ; Yaakob, Zahira ; Jali, Norazrina Mat ; Khadem, Dariush Jafar ; Wan Daud, Wan Ramli ; Herianto, Edy. / Influence of iron oxide nano particles on electrospun poly (vinylidene fluride)-based carbon nanofibers on hydrogen storage. Key Engineering Materials. Vol. 471-472 2011. pp. 1184-1189 (Key Engineering Materials).
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