Abstract
Hydroxy-ether-PO0 was synthesised via alcoholysis reaction of epoxidized palm olein (EPO0). The experimental design was conducted using response surface methodology (RSM) based on 3 factors; reaction time, reaction temperature and catalyst loading. Responses such as percentage of conversion and percentage of yield were determined using statistical software 'Design Expert 9'. Hydroxy-ether-PO0 showed the presence of proton peak attached to the carbon of ether (3.2, 3.5 ppm) and proton of the hydroxyl (4.8 ppm). The presence of carbon peak bonded to hydroxyl was detected at chemical shift 75 ppm and carbonyl carbon of ether at 72 ppm.
| Original language | English |
|---|---|
| Pages (from-to) | 1149-1154 |
| Number of pages | 6 |
| Journal | Sains Malaysiana |
| Volume | 45 |
| Issue number | 7 |
| Publication status | Published - 1 Jul 2016 |
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Keywords
- Alcoholysis
- Oxirane cleavage
- Palm olein
- Response surface methods
ASJC Scopus subject areas
- General
Cite this
Experimental design using response surface methods for palm olein-based hydroxy-ether systhesis. / Derawi, Darfizzi.
In: Sains Malaysiana, Vol. 45, No. 7, 01.07.2016, p. 1149-1154.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Experimental design using response surface methods for palm olein-based hydroxy-ether systhesis
AU - Derawi, Darfizzi
PY - 2016/7/1
Y1 - 2016/7/1
N2 - Hydroxy-ether-PO0 was synthesised via alcoholysis reaction of epoxidized palm olein (EPO0). The experimental design was conducted using response surface methodology (RSM) based on 3 factors; reaction time, reaction temperature and catalyst loading. Responses such as percentage of conversion and percentage of yield were determined using statistical software 'Design Expert 9'. Hydroxy-ether-PO0 showed the presence of proton peak attached to the carbon of ether (3.2, 3.5 ppm) and proton of the hydroxyl (4.8 ppm). The presence of carbon peak bonded to hydroxyl was detected at chemical shift 75 ppm and carbonyl carbon of ether at 72 ppm.
AB - Hydroxy-ether-PO0 was synthesised via alcoholysis reaction of epoxidized palm olein (EPO0). The experimental design was conducted using response surface methodology (RSM) based on 3 factors; reaction time, reaction temperature and catalyst loading. Responses such as percentage of conversion and percentage of yield were determined using statistical software 'Design Expert 9'. Hydroxy-ether-PO0 showed the presence of proton peak attached to the carbon of ether (3.2, 3.5 ppm) and proton of the hydroxyl (4.8 ppm). The presence of carbon peak bonded to hydroxyl was detected at chemical shift 75 ppm and carbonyl carbon of ether at 72 ppm.
KW - Alcoholysis
KW - Oxirane cleavage
KW - Palm olein
KW - Response surface methods
UR - http://www.scopus.com/inward/record.url?scp=84983334798&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=84983334798&partnerID=8YFLogxK
M3 - Article
VL - 45
SP - 1149
EP - 1154
JO - Sains Malaysiana
JF - Sains Malaysiana
SN - 0126-6039
IS - 7
ER -