Electrosynthesis and characterization of Cu(OH)<inf>2</inf> nanoparticle using Cu and Cu-PVC electrodes in alkaline solution

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11 Citations (Scopus)

Abstract

Cu(OH)<inf>2</inf> have been synthesized by electrochemistry technique using Cu and Cu-PVC electrodes in alkaline solution. The electrolysis process was carried out in 0.1 M KOH supporting electrode at room temperature. Experiments were performed in a three electrodes system using Cu and Cu-PVC as a working electrode, SCE as reference electrode and platinum wire as the counter electrode. The electrolysis of was performed using potential constant (1050 mV) in 50 mL capacity glass electrochemical cell. Universal Pulsa Dynamic EIS, Cyclic Voltammetry, Voltalab potentiostat (Model PGZ 402) was used for electrochemical behavior measurements. XRD and XPS have been used to characterize the morphology, structure, and composition of the compounds at electrode surface. The results of this experiment shown the Cu(OH)<inf>2</inf> is main product and higher purity. The advantages of our method for the Cu(OH)<inf>2</inf> synthesis are low temperature, simple, inexpensive, non-toxic raw materials and environmentally friendly.

Original languageEnglish
Pages (from-to)4911-4921
Number of pages11
JournalInternational Journal of Electrochemical Science
Volume10
Issue number6
Publication statusPublished - 2015

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Polyvinyl Chloride
Polyvinyl chlorides
Nanoparticles
Electrodes
Electrolysis
Electrochemical cells
Electrochemistry
cupric hydroxide
Platinum
Cyclic voltammetry
Raw materials
X ray photoelectron spectroscopy
Experiments
Wire
Glass
Temperature
Chemical analysis

Keywords

  • Alkaline solution
  • Cu and Cu-PVC
  • Cu(OH)<inf>2</inf>
  • Electrosynthesis
  • Nanoparticle

ASJC Scopus subject areas

  • Electrochemistry

Cite this

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title = "Electrosynthesis and characterization of Cu(OH)2 nanoparticle using Cu and Cu-PVC electrodes in alkaline solution",
abstract = "Cu(OH)2 have been synthesized by electrochemistry technique using Cu and Cu-PVC electrodes in alkaline solution. The electrolysis process was carried out in 0.1 M KOH supporting electrode at room temperature. Experiments were performed in a three electrodes system using Cu and Cu-PVC as a working electrode, SCE as reference electrode and platinum wire as the counter electrode. The electrolysis of was performed using potential constant (1050 mV) in 50 mL capacity glass electrochemical cell. Universal Pulsa Dynamic EIS, Cyclic Voltammetry, Voltalab potentiostat (Model PGZ 402) was used for electrochemical behavior measurements. XRD and XPS have been used to characterize the morphology, structure, and composition of the compounds at electrode surface. The results of this experiment shown the Cu(OH)2 is main product and higher purity. The advantages of our method for the Cu(OH)2 synthesis are low temperature, simple, inexpensive, non-toxic raw materials and environmentally friendly.",
keywords = "Alkaline solution, Cu and Cu-PVC, Cu(OH)<inf>2</inf>, Electrosynthesis, Nanoparticle",
author = "Riyanto and Othman, {Mohamed Rozali}",
year = "2015",
language = "English",
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journal = "International Journal of Electrochemical Science",
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TY - JOUR

T1 - Electrosynthesis and characterization of Cu(OH)2 nanoparticle using Cu and Cu-PVC electrodes in alkaline solution

AU - Riyanto,

AU - Othman, Mohamed Rozali

PY - 2015

Y1 - 2015

N2 - Cu(OH)2 have been synthesized by electrochemistry technique using Cu and Cu-PVC electrodes in alkaline solution. The electrolysis process was carried out in 0.1 M KOH supporting electrode at room temperature. Experiments were performed in a three electrodes system using Cu and Cu-PVC as a working electrode, SCE as reference electrode and platinum wire as the counter electrode. The electrolysis of was performed using potential constant (1050 mV) in 50 mL capacity glass electrochemical cell. Universal Pulsa Dynamic EIS, Cyclic Voltammetry, Voltalab potentiostat (Model PGZ 402) was used for electrochemical behavior measurements. XRD and XPS have been used to characterize the morphology, structure, and composition of the compounds at electrode surface. The results of this experiment shown the Cu(OH)2 is main product and higher purity. The advantages of our method for the Cu(OH)2 synthesis are low temperature, simple, inexpensive, non-toxic raw materials and environmentally friendly.

AB - Cu(OH)2 have been synthesized by electrochemistry technique using Cu and Cu-PVC electrodes in alkaline solution. The electrolysis process was carried out in 0.1 M KOH supporting electrode at room temperature. Experiments were performed in a three electrodes system using Cu and Cu-PVC as a working electrode, SCE as reference electrode and platinum wire as the counter electrode. The electrolysis of was performed using potential constant (1050 mV) in 50 mL capacity glass electrochemical cell. Universal Pulsa Dynamic EIS, Cyclic Voltammetry, Voltalab potentiostat (Model PGZ 402) was used for electrochemical behavior measurements. XRD and XPS have been used to characterize the morphology, structure, and composition of the compounds at electrode surface. The results of this experiment shown the Cu(OH)2 is main product and higher purity. The advantages of our method for the Cu(OH)2 synthesis are low temperature, simple, inexpensive, non-toxic raw materials and environmentally friendly.

KW - Alkaline solution

KW - Cu and Cu-PVC

KW - Cu(OH)<inf>2</inf>

KW - Electrosynthesis

KW - Nanoparticle

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