Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films

Ibtisam Yahya Abdullah, Muhammad Yahaya, Mohammad Hafizuddin Jumali, Haider Mohammed Shanshool

Research output: Chapter in Book/Report/Conference proceedingConference contribution

7 Citations (Scopus)

Abstract

This work reports the initial study on the effect of annealing process on the crystalline phase of poly(vinylidene fluoride) (PVDF) thin film. PVDF powder was dissolved in N,N-dimethylformamide before spincoated onto a glass substrate to form a film. The films were annealed at 30°C, 90°C and 110°C for 5 hrs. The crystalline phase of the powder PVDF as received was investigated by using XRD and FTIR techniques. Moreover, the crystalline phases of thin films after annealing were investigated by using the same techniques. XRD analysis showed that in powder form PVDF exists in α-phase. Each annealed PVDF thin films exhibited identical formation of three-phases material namely γ (as major phase) while α and β phases as the minor phases. The FTIR analysis showed that the powder form of PVDF exists in α and β phases. FTIR measurement further confirmed the XRD results implying that the annealing process has no significant effect on the phase formation in PVDF films.

Original languageEnglish
Title of host publication2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium
EditorsZahari Ibrahim, Haja Maideen Kader Maideen, Nazlina Ibrahim, Nurul Huda Abd Karim, Taufik Yusof, Fatimah Abdul Razak, Nurulkamal Maseran, Rozida Mohd Khalid, Noor Baa'yah Ibrahim, Hasidah Mohd. Sidek, Mohd Salmi Md Noorani, Norbert Simon
PublisherAmerican Institute of Physics Inc.
Pages147-151
Number of pages5
ISBN (Electronic)9780735412507
DOIs
Publication statusPublished - 1 Jan 2014
Event2014 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2014 - Selangor, Malaysia
Duration: 9 Apr 201411 Apr 2014

Publication series

NameAIP Conference Proceedings
Volume1614
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Other

Other2014 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2014
CountryMalaysia
CitySelangor
Period9/4/1411/4/14

Fingerprint

vinylidene
fluorides
annealing
thin films
glass

Keywords

  • Crystalline phase
  • FTIR
  • Piezoelectric
  • Spin-coated
  • XRD

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Abdullah, I. Y., Yahaya, M., Jumali, M. H., & Shanshool, H. M. (2014). Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films. In Z. Ibrahim, H. M. K. Maideen, N. Ibrahim, N. H. A. Karim, T. Yusof, F. A. Razak, N. Maseran, R. M. Khalid, N. B. Ibrahim, H. M. Sidek, M. S. M. Noorani, ... N. Simon (Eds.), 2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium (pp. 147-151). (AIP Conference Proceedings; Vol. 1614). American Institute of Physics Inc.. https://doi.org/10.1063/1.4895187

Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films. / Abdullah, Ibtisam Yahya; Yahaya, Muhammad; Jumali, Mohammad Hafizuddin; Shanshool, Haider Mohammed.

2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium. ed. / Zahari Ibrahim; Haja Maideen Kader Maideen; Nazlina Ibrahim; Nurul Huda Abd Karim; Taufik Yusof; Fatimah Abdul Razak; Nurulkamal Maseran; Rozida Mohd Khalid; Noor Baa'yah Ibrahim; Hasidah Mohd. Sidek; Mohd Salmi Md Noorani; Norbert Simon. American Institute of Physics Inc., 2014. p. 147-151 (AIP Conference Proceedings; Vol. 1614).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abdullah, IY, Yahaya, M, Jumali, MH & Shanshool, HM 2014, Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films. in Z Ibrahim, HMK Maideen, N Ibrahim, NHA Karim, T Yusof, FA Razak, N Maseran, RM Khalid, NB Ibrahim, HM Sidek, MSM Noorani & N Simon (eds), 2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium. AIP Conference Proceedings, vol. 1614, American Institute of Physics Inc., pp. 147-151, 2014 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2014, Selangor, Malaysia, 9/4/14. https://doi.org/10.1063/1.4895187
Abdullah IY, Yahaya M, Jumali MH, Shanshool HM. Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films. In Ibrahim Z, Maideen HMK, Ibrahim N, Karim NHA, Yusof T, Razak FA, Maseran N, Khalid RM, Ibrahim NB, Sidek HM, Noorani MSM, Simon N, editors, 2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium. American Institute of Physics Inc. 2014. p. 147-151. (AIP Conference Proceedings). https://doi.org/10.1063/1.4895187
Abdullah, Ibtisam Yahya ; Yahaya, Muhammad ; Jumali, Mohammad Hafizuddin ; Shanshool, Haider Mohammed. / Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films. 2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium. editor / Zahari Ibrahim ; Haja Maideen Kader Maideen ; Nazlina Ibrahim ; Nurul Huda Abd Karim ; Taufik Yusof ; Fatimah Abdul Razak ; Nurulkamal Maseran ; Rozida Mohd Khalid ; Noor Baa'yah Ibrahim ; Hasidah Mohd. Sidek ; Mohd Salmi Md Noorani ; Norbert Simon. American Institute of Physics Inc., 2014. pp. 147-151 (AIP Conference Proceedings).
@inproceedings{ae341da4446b49889aaea4b7923590ae,
title = "Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films",
abstract = "This work reports the initial study on the effect of annealing process on the crystalline phase of poly(vinylidene fluoride) (PVDF) thin film. PVDF powder was dissolved in N,N-dimethylformamide before spincoated onto a glass substrate to form a film. The films were annealed at 30°C, 90°C and 110°C for 5 hrs. The crystalline phase of the powder PVDF as received was investigated by using XRD and FTIR techniques. Moreover, the crystalline phases of thin films after annealing were investigated by using the same techniques. XRD analysis showed that in powder form PVDF exists in α-phase. Each annealed PVDF thin films exhibited identical formation of three-phases material namely γ (as major phase) while α and β phases as the minor phases. The FTIR analysis showed that the powder form of PVDF exists in α and β phases. FTIR measurement further confirmed the XRD results implying that the annealing process has no significant effect on the phase formation in PVDF films.",
keywords = "Crystalline phase, FTIR, Piezoelectric, Spin-coated, XRD",
author = "Abdullah, {Ibtisam Yahya} and Muhammad Yahaya and Jumali, {Mohammad Hafizuddin} and Shanshool, {Haider Mohammed}",
year = "2014",
month = "1",
day = "1",
doi = "10.1063/1.4895187",
language = "English",
series = "AIP Conference Proceedings",
publisher = "American Institute of Physics Inc.",
pages = "147--151",
editor = "Zahari Ibrahim and Maideen, {Haja Maideen Kader} and Nazlina Ibrahim and Karim, {Nurul Huda Abd} and Taufik Yusof and Razak, {Fatimah Abdul} and Nurulkamal Maseran and Khalid, {Rozida Mohd} and Ibrahim, {Noor Baa'yah} and Sidek, {Hasidah Mohd.} and Noorani, {Mohd Salmi Md} and Norbert Simon",
booktitle = "2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium",

}

TY - GEN

T1 - Effect of annealing process on the phase formation in Poly(vinylidene fluoride) thin films

AU - Abdullah, Ibtisam Yahya

AU - Yahaya, Muhammad

AU - Jumali, Mohammad Hafizuddin

AU - Shanshool, Haider Mohammed

PY - 2014/1/1

Y1 - 2014/1/1

N2 - This work reports the initial study on the effect of annealing process on the crystalline phase of poly(vinylidene fluoride) (PVDF) thin film. PVDF powder was dissolved in N,N-dimethylformamide before spincoated onto a glass substrate to form a film. The films were annealed at 30°C, 90°C and 110°C for 5 hrs. The crystalline phase of the powder PVDF as received was investigated by using XRD and FTIR techniques. Moreover, the crystalline phases of thin films after annealing were investigated by using the same techniques. XRD analysis showed that in powder form PVDF exists in α-phase. Each annealed PVDF thin films exhibited identical formation of three-phases material namely γ (as major phase) while α and β phases as the minor phases. The FTIR analysis showed that the powder form of PVDF exists in α and β phases. FTIR measurement further confirmed the XRD results implying that the annealing process has no significant effect on the phase formation in PVDF films.

AB - This work reports the initial study on the effect of annealing process on the crystalline phase of poly(vinylidene fluoride) (PVDF) thin film. PVDF powder was dissolved in N,N-dimethylformamide before spincoated onto a glass substrate to form a film. The films were annealed at 30°C, 90°C and 110°C for 5 hrs. The crystalline phase of the powder PVDF as received was investigated by using XRD and FTIR techniques. Moreover, the crystalline phases of thin films after annealing were investigated by using the same techniques. XRD analysis showed that in powder form PVDF exists in α-phase. Each annealed PVDF thin films exhibited identical formation of three-phases material namely γ (as major phase) while α and β phases as the minor phases. The FTIR analysis showed that the powder form of PVDF exists in α and β phases. FTIR measurement further confirmed the XRD results implying that the annealing process has no significant effect on the phase formation in PVDF films.

KW - Crystalline phase

KW - FTIR

KW - Piezoelectric

KW - Spin-coated

KW - XRD

UR - http://www.scopus.com/inward/record.url?scp=85053404058&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=85053404058&partnerID=8YFLogxK

U2 - 10.1063/1.4895187

DO - 10.1063/1.4895187

M3 - Conference contribution

AN - SCOPUS:85053404058

T3 - AIP Conference Proceedings

SP - 147

EP - 151

BT - 2014 UKM FST Postgraduate Colloquium - Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2014 Postgraduate Colloquium

A2 - Ibrahim, Zahari

A2 - Maideen, Haja Maideen Kader

A2 - Ibrahim, Nazlina

A2 - Karim, Nurul Huda Abd

A2 - Yusof, Taufik

A2 - Razak, Fatimah Abdul

A2 - Maseran, Nurulkamal

A2 - Khalid, Rozida Mohd

A2 - Ibrahim, Noor Baa'yah

A2 - Sidek, Hasidah Mohd.

A2 - Noorani, Mohd Salmi Md

A2 - Simon, Norbert

PB - American Institute of Physics Inc.

ER -