Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies

Muhammad Nur Adeel Nordin, Muhammad Hamiz Zafran Zakaria, Nurul Nadiha Mohd Kamrin, Maratun Najiha Abu Tahari, Mohd. Ambar Yarmo

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

Commercially available porous silica gel (SG) is chemically modified for carbon dioxide capture. Calcinated silica gel functionalized with amine (tetradecylamine, TDA) using wet impregnation has been employed as a porous media. The prepared adsorbents is characterized by x-ray diffractometry (XRD) and N2 physisorption techniques (Brunauer-Emmet-Teller analysis, BET). Appearance of 3 new crystalline peaks on 65TDA/SG diffractogram evidenced the presence of TDA molecules on the SG. Significant changes in physical properties of the adsorbents further ascertained the dispersion of TDA on the internal channels and external surface of the SG.

Original languageEnglish
Title of host publicationCurrent Material Research Using X-Rays and Related Techniques II
PublisherTrans Tech Publications Ltd
Pages175-178
Number of pages4
Volume888 MSF
ISBN (Print)9783035710298
DOIs
Publication statusPublished - 2017
EventInternational Conference on X-Rays and Related Techniques in Research and Industry, ICXRI 2016 - Putrajaya, Malaysia
Duration: 17 Aug 201618 Aug 2016

Publication series

NameMaterials Science Forum
Volume888 MSF
ISSN (Print)02555476

Other

OtherInternational Conference on X-Rays and Related Techniques in Research and Industry, ICXRI 2016
CountryMalaysia
CityPutrajaya
Period17/8/1618/8/16

Fingerprint

Silica Gel
Silica gel
silica gel
X ray diffraction analysis
adsorbents
x rays
Adsorbents
Physisorption
Carbon Dioxide
Impregnation
Amines
Porous materials
carbon dioxide
Carbon dioxide
amines
Physical properties
physical properties
Crystalline materials
X rays
Molecules

Keywords

  • CO capture
  • Modified SG
  • TDA impregnation

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Nordin, M. N. A., Zakaria, M. H. Z., Mohd Kamrin, N. N., Abu Tahari, M. N., & Yarmo, M. A. (2017). Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies. In Current Material Research Using X-Rays and Related Techniques II (Vol. 888 MSF, pp. 175-178). (Materials Science Forum; Vol. 888 MSF). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.888.175

Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies. / Nordin, Muhammad Nur Adeel; Zakaria, Muhammad Hamiz Zafran; Mohd Kamrin, Nurul Nadiha; Abu Tahari, Maratun Najiha; Yarmo, Mohd. Ambar.

Current Material Research Using X-Rays and Related Techniques II. Vol. 888 MSF Trans Tech Publications Ltd, 2017. p. 175-178 (Materials Science Forum; Vol. 888 MSF).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Nordin, MNA, Zakaria, MHZ, Mohd Kamrin, NN, Abu Tahari, MN & Yarmo, MA 2017, Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies. in Current Material Research Using X-Rays and Related Techniques II. vol. 888 MSF, Materials Science Forum, vol. 888 MSF, Trans Tech Publications Ltd, pp. 175-178, International Conference on X-Rays and Related Techniques in Research and Industry, ICXRI 2016, Putrajaya, Malaysia, 17/8/16. https://doi.org/10.4028/www.scientific.net/MSF.888.175
Nordin MNA, Zakaria MHZ, Mohd Kamrin NN, Abu Tahari MN, Yarmo MA. Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies. In Current Material Research Using X-Rays and Related Techniques II. Vol. 888 MSF. Trans Tech Publications Ltd. 2017. p. 175-178. (Materials Science Forum). https://doi.org/10.4028/www.scientific.net/MSF.888.175
Nordin, Muhammad Nur Adeel ; Zakaria, Muhammad Hamiz Zafran ; Mohd Kamrin, Nurul Nadiha ; Abu Tahari, Maratun Najiha ; Yarmo, Mohd. Ambar. / Characterization of silica gel impregnated with tetradecylamine by X-ray diffractometry and Brunauer-Emmet-Teller studies. Current Material Research Using X-Rays and Related Techniques II. Vol. 888 MSF Trans Tech Publications Ltd, 2017. pp. 175-178 (Materials Science Forum).
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