3-Methyl-2-propionamido-butanoic acid

Bohari Mohd. Yamin, Eliyanti A. Othman

Research output: Contribution to journalArticle

Abstract

The reaction of propionyl isothio-cyanate with valine was found to give the title compound, C8H15NO3, instead of the expected thio-urea product. The whole mol-ecule is non-planar and the carbonyl group is cis to the methyl-butanoic acid group across the C - N bond. Inter-molecular O - H⋯O and N - H⋯O hydrogen bonds build up a two-dimensional network developing parallel to (100).

Original languageEnglish
JournalActa Crystallographica Section E: Structure Reports Online
Volume65
Issue number4
DOIs
Publication statusPublished - 2009

Fingerprint

Cyanates
Butyric acid
Butyric Acid
Valine
Urea
Hydrogen bonds
cyanates
acids
ureas
hydrogen bonds
products

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Materials Science(all)
  • Chemistry(all)

Cite this

3-Methyl-2-propionamido-butanoic acid. / Mohd. Yamin, Bohari; Othman, Eliyanti A.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 65, No. 4, 2009.

Research output: Contribution to journalArticle

Mohd. Yamin, Bohari ; Othman, Eliyanti A. / 3-Methyl-2-propionamido-butanoic acid. In: Acta Crystallographica Section E: Structure Reports Online. 2009 ; Vol. 65, No. 4.
@article{a104524950924381a9a5e3df0ef4b102,
title = "3-Methyl-2-propionamido-butanoic acid",
abstract = "The reaction of propionyl isothio-cyanate with valine was found to give the title compound, C8H15NO3, instead of the expected thio-urea product. The whole mol-ecule is non-planar and the carbonyl group is cis to the methyl-butanoic acid group across the C - N bond. Inter-molecular O - H⋯O and N - H⋯O hydrogen bonds build up a two-dimensional network developing parallel to (100).",
author = "{Mohd. Yamin}, Bohari and Othman, {Eliyanti A.}",
year = "2009",
doi = "10.1107/S1600536809007119",
language = "English",
volume = "65",
journal = "Acta Crystallographica Section E: Structure Reports Online",
issn = "1600-5368",
publisher = "International Union of Crystallography",
number = "4",

}

TY - JOUR

T1 - 3-Methyl-2-propionamido-butanoic acid

AU - Mohd. Yamin, Bohari

AU - Othman, Eliyanti A.

PY - 2009

Y1 - 2009

N2 - The reaction of propionyl isothio-cyanate with valine was found to give the title compound, C8H15NO3, instead of the expected thio-urea product. The whole mol-ecule is non-planar and the carbonyl group is cis to the methyl-butanoic acid group across the C - N bond. Inter-molecular O - H⋯O and N - H⋯O hydrogen bonds build up a two-dimensional network developing parallel to (100).

AB - The reaction of propionyl isothio-cyanate with valine was found to give the title compound, C8H15NO3, instead of the expected thio-urea product. The whole mol-ecule is non-planar and the carbonyl group is cis to the methyl-butanoic acid group across the C - N bond. Inter-molecular O - H⋯O and N - H⋯O hydrogen bonds build up a two-dimensional network developing parallel to (100).

UR - http://www.scopus.com/inward/record.url?scp=64149120681&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=64149120681&partnerID=8YFLogxK

U2 - 10.1107/S1600536809007119

DO - 10.1107/S1600536809007119

M3 - Article

C2 - 21582407

AN - SCOPUS:64149120681

VL - 65

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

SN - 1600-5368

IS - 4

ER -